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HRID1174575

反应详情

EQUATION

反应方程式

HRID 1174575 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CC(C)=CCn1c(N2CC3CN(C(=O)OC(C)(C)C)CC3C2)nc2c1c(=O)n(CC(=O)c1ccccc1)c(=O)n2C
HCID68688281

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)=CCn1c(N2C[C@H]3CNC[C@H]3C2)nc2c1c(=O)n(CC(=O)c1ccccc1)c(=O)n2C.Cl
HCID68690226

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

2 次

PROCEDURE

实验过程

This compound was obtained by dissolving 50 mg of tert-butyl 5-[3-methyl-7-(3-methyl-but-2-enyl)-2,6-dioxo-1-(2-oxo-2-phenyl-ethyl)-2,3,6,7-tetrahydro-1H-purin-8-yl]-hexahydropyrrolo[3,4-c]pyrrole-2-carboxylate in 5 ml of ethyl acetate, treating the solution with excess hydrogen chloride solution in ethyl acetate, concentrating in a rotary evaporator and stirring with diisopropyl ether.

WORKUP

后处理

  1. customThis compound was obtained
  2. concentrationconcentrating in a rotary evaporator