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HRID1180061

反应详情

EQUATION

反应方程式

HRID 1180061 的结构方程式

REACTANTS

反应物

2
结构：Oc1cccnc1
HCID7971

3-Pyridinol

C5H5NO

结构：CN(C(=O)Oc1ccc(CO)cc1)c1ccccc1
HCID69518671

未命名化合物

PRODUCTS

生成物

1
结构：CN(C(=O)Oc1ccc(COc2cccnc2)cc1)c1ccccc1
HCID69519278

未命名化合物

收率 43%

PROCEDURE

实验过程

The title compound was prepared in 43% yield as an oil using methyl-phenyl-carbamic acid 4-hydroxymethyl-phenyl ester and 3-hydroxypyridine. 1H NMR (400 MHz; CDCl3): δ 3.44 (br s, 3H), 5.12 (s, 2H), 7.17 (br s, 2H), 7.27-7.46 (m, 9H), 8.29 (br s, 1H), 8.49 (br s, 1H); HPLC-MS: m/z=335.0 (M+1); Rt=2.74 min.