HRID1183000

反应详情

EQUATION

反应方程式

HRID 1183000 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

610 mg (1.62 mmol) of tert-butyl 3-[(6-amino-5-nitropyridin-2-yl)-amino]piperidine-1-carboxylate (Example 14A) were dissolved in 40 ml of a hydrochloric acid solution in dioxane (4 M) and stirred at RT for 30 min. On completion of reaction, the solvent was removed completely. 662 mg of the crude product were obtained.

WORKUP

后处理

  1. customOn completion of reaction
  2. customthe solvent was removed completely