HRID1184608
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of the product from Example 174E (1.10 g, 2.71 mmol) in dichloromethane (3 mL) was treated with hydrochloric acid in 1,4-dioxane (4 M, 3 mL). The mixture was stirred for 30 minutes, during which time a solid formed. The volatiles were removed in vacuo to give the title compound.
WORKUP
后处理
- customformed
- customThe volatiles were removed in vacuo