HRID1185438

反应详情

EQUATION

反应方程式

HRID 1185438 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To 40 ml of a saturated solution of hydrochloric acid in ethanol 2 g of 2-Furan-2-yl-quinoline-4-carboxylic acid was added and the mixture was heated to reflux for 3 h. Then, after cooling to RT, 30 ml of toluene was added and the solvents were removed under reduced pressure. The obtained crude product was pure enough for the next reaction step. Yield: 2.5 g.

WORKUP

后处理

  1. temperaturethe mixture was heated
  2. temperatureto reflux for 3 h
  3. customthe solvents were removed under reduced pressure
  4. customThe obtained crude product
  5. customwas pure enough for the next reaction step