HRID1185574

反应详情

EQUATION

反应方程式

HRID 1185574 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a solution of 739 mg 4-[(S)-2-tert-Butoxycarbonylamino-3-(1H-[1,2,3]triazol-4-yl)-propionyl]-piperazine-1-carboxylic acid butyl ester in 8 ml dichloromethane were added 1.3 ml TFA. After 12 h stirring at RT the solvents were removed and the residue was codistilled twice with toluene. Yield: 1.32 g.

WORKUP

后处理

  1. customwere removed