Iodoethane → HCID 66736185, compound

HRID 1187908Notes

Reaction equation

[Br:1][C:2]1[CH:7]=[C:6]([CH3:8])[NH:5][C:4](=[O:9])[CH:3]=1.[CH2:10](I)[CH3:11].C([O-])([O-])=O.[K+].[K+]>>[Br:1][C:2]1[CH:7]=[C:6]([CH3:8])[N:5]([CH2:10][CH3:11])[C:4](=[O:9])[CH:3]=1

Participants

Reactant 3

HCID 6340Iodoethane

HCID 11430Potassium Carbonate

HCID 231494724-Bromo-6-methylpyridin-2-ol

Product 1

HCID 66736185HCID 66736185, compound

Procedure

4-bromo-1-ethyl-6-methylpyridin-2(1H)-one was prepared by alkylation of 4-bromo-6-methylpyridin-2(1H)-one with ethyl iodide using K2CO3 following a procedure analogous to that described in Example 59 Step 1.

Sources & evidence

ORD record: ord-7085d60e551d427993443f2d4ae0cee0
Source dataset: uspto-grants-2014_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08673899B2

Reaction notes

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