HRID1189652

反应详情

EQUATION

反应方程式

HRID 1189652 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of ethyl-2-[4-trifluoromethyl-piperidinyl]-4-methylamino-5-nitro-benzoate (380 mg, 1.01 mmol), Ra—Ni (500 mg) and THF (20 mL) is stirred overnight under 10 bar H2-atmosphere. The mixture is filtered, and the filtrate is concentrated.

WORKUP

后处理

  1. filtrationThe mixture is filtered
  2. concentrationthe filtrate is concentrated