反应详情

Reaction of TBPA with MIPA gives an TBPA/MIPA adduct. TBPA is sold in commerce by Albermarle as Saytex® RB-49. MIPA is sold in commerce by Dow Chemical. 44.8 mmol of TBPA is added to a round bottom flask with 50.74 grams of ethanol. The mixture is heated to reflux after which 44.8 mmol of MIPA is added dropwise and the solution refluxed for 1 hour. The ethanol is removed using a rotary evaporator to produce a yellow crystalline solid.