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HRID1194291

反应详情

EQUATION

反应方程式

HRID 1194291 的结构方程式

REACTANTS

反应物

3
结构：COc1ccccc1
HCID7519

Anisole

C7H8O

结构：COS(=O)(=O)C(F)(F)F
HCID9526

Methyl trifluoromethanesulfonate

C2H3F3O3S

结构：COc1nc2cccccc-2n1
HCID20064381

2-Methoxycyclohepta[d]imidazole

C9H8N2O

PRODUCTS

生成物

1
结构：COC1[NH+]=C2C=CC=CC=C2N1C.O=S(=O)([O-])C(F)(F)F
HCID178494296

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

First, 0.9 g of 2-methoxycycloheptimidazole was added to 5 ml of anisole, and 1.1 g of methyl trifluoromethanesulfonate was added dropwise. After being stirred at room temperature for one hour, 30 ml of ethyl acetate was added, and deposited crystals were collected by filtration and dried.

WORKUP

后处理

  1. additionwas added dropwise
  2. filtrationwere collected by filtration
  3. customdried