Epichlorohydrin → HCID 135976877, compound

HRID 1195689Notes

Reaction equation

HRID 1195689 reaction equation
C1([CH:7]([N:14]2[CH2:19][CH2:18]NCC2)[C:8]2[CH:13]=[CH:12]C=CC=2)C=CC=CC=1.[CH2:20]([CH:22]1[O:24][CH2:23]1)Cl.[CH2:25](N(CC)CC)C>CC(C)=O>[OH:24][C:23]1[CH:18]=[C:19]2[C:12]([CH:13]=[CH:8][CH:7]=[N:14]2)=[CH:20][C:22]=1[CH3:25]

Participants

5

Reactant 3

HCID 7835EpichlorohydrinHCID 8471TriethylamineHCID 70048Benzhydrylpiperazine

Product 1

HCID 135976877HCID 135976877, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

In 50 ml of acetone were dissolved 5.04 g of diphenylmethylpiperazine and 5.5 g of epichlorohydrin, and 4.2 ml of triethylamine was then added thereto.

Workup

  1. additionwas then added

Sources & evidence

ORD record
ord-812ae7db1b7c420295945351fe826d31
Source dataset
uspto-grants-1992_05
Patent number
US05112817

Reaction notes

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