HRID1196506

反应详情

EQUATION

反应方程式

HRID 1196506 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of the product of stage (iii) (5.50 g) in ethyl acetate (60 ml) was hydrogenated over 10% palladium on carbon (0.50 g) for 4 h. The catalyst was filtered off and the filtrate evaporated in vacuo to give the title compound as an oil (3.0 g).

WORKUP

后处理

  1. filtrationThe catalyst was filtered off
  2. customthe filtrate evaporated in vacuo