1-Propanol → HCID 19896179, compound

HRID 1196752Notes

Reaction equation

HRID 1196752 reaction equation
C([O:3][CH:4]([O:8][CH2:9][CH3:10])[CH:5]([Cl:7])[Cl:6])C.C[C:12]1[CH:17]=[CH:16]C(S(O)(=O)=O)=CC=1.[CH2:22](O)CC>>[CH2:9]([O:8][CH:4]([O:3][CH2:16][CH2:17][CH3:12])[CH:5]([Cl:6])[Cl:7])[CH2:10][CH3:22]

Participants

4

Reactant 3

HCID 10311-PropanolHCID 6101p-Toluenesulfonic acidHCID 120801,1-Dichloro-2,2-diethoxyethane

Product 1

HCID 19896179HCID 19896179, compound

Procedure

A mixture of 5 g of dichloro-acetaldehyde diethyl-acetal, 30 ml of propanol and 0.1 g of 4-methyl-benzene-sulphonic acid is heated on a water-bath for 5 hours, then distilled.

Workup

  1. temperatureis heated on a water-bath for 5 hours
  2. distillationdistilled

Sources & evidence

ORD record
ord-e5add924536742ae9cf71aad2fb78cfe
Source dataset
uspto-grants-1992_05
Patent number
US05116402

Reaction notes

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