p-Anisoyl chloride → HCID 14983036, compound

HRID 1197956Notes

Reaction equation

HRID 1197956 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[CH3:12][O:13][C:14]1[CH:22]=[CH:21][C:17]([C:18](Cl)=O)=[CH:16][CH:15]=1.Br[CH2:24][CH2:25][CH2:26][CH2:27][CH2:28]Cl.[OH:30][CH:31]1[CH2:36][CH2:35][NH:34][CH2:33][CH2:32]1>>[OH:30][CH:31]1[CH2:36][CH2:35][N:34]([CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][O:8][C:5]2[CH:6]=[CH:7][C:2]3[O:1][C:18]([C:17]4[CH:21]=[CH:22][C:14]([O:13][CH3:12])=[CH:15][CH:16]=4)=[CH:10][C:9](=[O:11])[C:3]=3[CH:4]=2)[CH2:33][CH2:32]1

Participants

5

Reactant 4

HCID 7477p-Anisoyl chlorideHCID 102792-AcetylhydroquinoneHCID 79341Piperidin-4-olHCID 960701-Bromo-5-chloropentane

Product 1

HCID 14983036HCID 14983036, compound

Procedure

The compound was prepared by a method similar to Example 11 from 2',5'-dihydroxyacetophenone, 4 -methoxybenzoyl chloride, 1-bromo-5-chloropentane, and 4-hydroxypiperidine: mp 138°-139° C.

Sources & evidence

ORD record
ord-563c94d95d204484a86b970864bb2eaa
Source dataset
uspto-grants-1994_01
Patent number
US05278174

Reaction notes

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