2-Acetylhydroquinone → HCID 14983029, compound

HRID 1197965Notes

Reaction equation

HRID 1197965 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[Cl:12][C:13]1[CH:14]=[C:15]([CH:19]=[CH:20][CH:21]=1)[C:16](Cl)=O.Br[CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28]Cl.[OH:30][CH:31]1[CH2:36][CH2:35][NH:34][CH2:33][CH2:32]1>>[Cl:12][C:13]1[CH:14]=[C:15]([C:16]2[O:1][C:2]3[CH:7]=[CH:6][C:5]([O:8][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][N:34]4[CH2:35][CH2:36][CH:31]([OH:30])[CH2:32][CH2:33]4)=[CH:4][C:3]=3[C:9](=[O:11])[CH:10]=2)[CH:19]=[CH:20][CH:21]=1

Participants

5

Reactant 4

HCID 102792-AcetylhydroquinoneHCID 69252Benzoyl chloride, 3-chloro-HCID 79341Piperidin-4-olHCID 805161-Bromo-6-chlorohexane

Product 1

HCID 14983029HCID 14983029, compound

Procedure

The compound was prepared by a method similar to Example 11 from 2',5'-dihydroxyacetophenone, 3-chlorobenzoyl chloride, 1-bromo-6-chlorohexane, and 4-hydroxypiperidine: mp 120°-121° C.

Sources & evidence

ORD record
ord-9946a72ac52948498e6b4b3439cd0aa4
Source dataset
uspto-grants-1994_01
Patent number
US05278174

Reaction notes

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