Piperidine → HCID 18959697, compound

HRID 1197966Notes

Reaction equation

HRID 1197966 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[CH:12]1([C:18]([Cl:20])=O)[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1.Br[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27]Cl.[NH:29]1[CH2:34][CH2:33][CH2:32][CH2:31][CH2:30]1>>[ClH:20].[CH:12]1([C:18]2[O:1][C:2]3[CH:7]=[CH:6][C:5]([O:8][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][N:29]4[CH2:34][CH2:33][CH2:32][CH2:31][CH2:30]4)=[CH:4][C:3]=3[C:9](=[O:11])[CH:10]=2)[CH2:17][CH2:16][CH2:15][CH2:14][CH2:13]1

Participants

5

Reactant 4

HCID 8082PiperidineHCID 102792-AcetylhydroquinoneHCID 75938Cyclohexanecarbonyl chlorideHCID 805161-Bromo-6-chlorohexane

Product 1

HCID 18959697HCID 18959697, compound

Procedure

The compound was prepared by a method similar to Example 11 from 2',5'-dihydroxyacetophenone, cyclohexanecarbonyl chloride, 1-bromo-6-chlorohexane, and piperidine: mp 164°-165° C.

Sources & evidence

ORD record
ord-87c6033d3e634404b5671847335f0fd3
Source dataset
uspto-grants-1994_01
Patent number
US05278174

Reaction notes

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