Piperidine → HCID 67691040, compound
Reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5](O)=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[CH:12]1([C:17]([Cl:19])=[O:18])[CH2:16][CH2:15][CH2:14][CH2:13]1.Br[CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26]Cl.[NH:28]1[CH2:33][CH2:32][CH2:31][CH2:30][CH2:29]1>>[ClH:19].[CH:25]1([C:26]2[O:1][C:2]3[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=3[C:9](=[O:11])[C:10]=2[O:18][CH2:17][CH2:12][CH2:16][CH2:15][CH2:14][CH2:13][CH:29]2[NH:28][CH2:33][CH2:32][CH2:31][CH2:30]2)[CH2:24][CH2:23][CH2:22][CH2:21]1Participants
5
Procedure
The compound was prepared by a method similar to Example 11 from 2',5'-dihydroxyacetophenone, cyclopentanecarbonyl chloride, 1-bromo-6-chlorohexane, and piperidine: mp 138°-139° C.
Sources & evidence
- ORD record
- ord-fdb08be8d44147d5bdfdcd8926d39fae
- Source dataset
- uspto-grants-1994_01
- Patent number
- US05278174
Reaction notes
Loading…