Piperidine → HCID 67691234, compound

HRID 1197972Notes

Reaction equation

HRID 1197972 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[CH:12]1([C:16]([Cl:18])=O)[CH2:15][CH2:14][CH2:13]1.Br[CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25]Cl.[NH:27]1[CH2:32][CH2:31][CH2:30][CH2:29][CH2:28]1>>[ClH:18].[CH:12]1([C:16]2[O:1][C:2]3[CH:7]=[CH:6][C:5]([O:8][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][N:27]4[CH2:32][CH2:31][CH2:30][CH2:29][CH2:28]4)=[CH:4][C:3]=3[C:9](=[O:11])[CH:10]=2)[CH2:15][CH2:14][CH2:13]1

Participants

5

Reactant 4

HCID 8082PiperidineHCID 102792-AcetylhydroquinoneHCID 78705Cyclobutanecarbonyl chlorideHCID 805161-Bromo-6-chlorohexane

Product 1

HCID 67691234HCID 67691234, compound

Procedure

The compound was prepared by a method similar to Example 11 from 2',5'-dihydroxyacetophenone, cyclobutanecarbonyl chloride, 1-bromo-6-chlorohexane, and piperidine: mp 165°-166° C.

Sources & evidence

ORD record
ord-d06e1dbdb21c4f64a81c9dcbab27349a
Source dataset
uspto-grants-1994_01
Patent number
US05278174

Reaction notes

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