Piperidine → HCID 18959724, compound

HRID 1197974Notes

Reaction equation

HRID 1197974 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5](O)=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[S:12]1[CH:16]=[CH:15][CH:14]=[C:13]1[C:17]([Cl:19])=O.BrCCCCCCCl.[NH:28]1[CH2:33][CH2:32][CH2:31][CH2:30][CH2:29]1>>[ClH:19].[N:28]1([C:5]2[CH:6]=[CH:7][C:2]3[O:1][C:17]([C:13]4[S:12][CH:16]=[CH:15][CH:14]=4)=[CH:10][C:9](=[O:11])[C:3]=3[CH:4]=2)[CH2:33][CH2:32][CH2:31][CH2:30][CH2:29]1

Participants

5

Reactant 4

HCID 8082PiperidineHCID 102792-AcetylhydroquinoneHCID 789282-Thiophenecarbonyl chlorideHCID 805161-Bromo-6-chlorohexane

Product 1

HCID 18959724HCID 18959724, compound

Procedure

The compound was prepared by a method similar to Example 11 from 2',5'-dihydroxyacetophenone, 2-thiophenecarbonyl chloride, 1-bromo-6-chlorohexane, and piperidine: mp 184°-185° C.

Sources & evidence

ORD record
ord-7457984f2f634fd9ab0a86d3ad705880
Source dataset
uspto-grants-1994_01
Patent number
US05278174

Reaction notes

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