Piperidine → HCID 67691868, compound

HRID 1197988Notes

Reaction equation

HRID 1197988 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[N:12]1[CH:17]=[CH:16][CH:15]=[C:14]([C:18]([Cl:20])=O)[CH:13]=1.Br[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27]Cl.[NH:29]1[CH2:34][CH2:33][CH2:32][CH2:31][CH2:30]1>>[ClH:20].[N:29]1([CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][O:8][C:5]2[CH:6]=[CH:7][C:2]3[O:1][C:18]([C:14]4[CH:13]=[N:12][CH:17]=[CH:16][CH:15]=4)=[CH:10][C:9](=[O:11])[C:3]=3[CH:4]=2)[CH2:34][CH2:33][CH2:32][CH2:31][CH2:30]1

Participants

5

Reactant 4

HCID 8082PiperidineHCID 102792-AcetylhydroquinoneHCID 805161-Bromo-6-chlorohexaneHCID 82604Nicotinoyl chloride

Product 1

HCID 67691868HCID 67691868, compound

Procedure

The compound was prepared by the method of Example 11 from 2',5'-dihydroxyacetophenone, 3-pyridylcarbonyl chloride, 1-bromo-6-chlorohexane, and piperidine: mp 192°-193° C.

Sources & evidence

ORD record
ord-1ee72597d3c442a5be602c51f179f836
Source dataset
uspto-grants-1994_01
Patent number
US05278174

Reaction notes

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