2-Acetylhydroquinone → HCID 18959699, compound

HRID 1197990Notes

Reaction equation

HRID 1197990 reaction equation
[OH:1][C:2]1[CH:7]=[CH:6][C:5]([OH:8])=[CH:4][C:3]=1[C:9](=[O:11])[CH3:10].[N:12]1[CH:17]=[CH:16][C:15]([C:18]([Cl:20])=O)=[CH:14][CH:13]=1.[OH:21][CH:22]1[CH2:27][CH2:26][NH:25][CH2:24][CH2:23]1>>[ClH:20].[OH:21][CH:22]1[CH2:27][CH2:26][N:25]([CH2:6][CH2:7][CH2:2][CH2:3][CH2:4][CH2:5][O:8][C:5]2[CH:6]=[CH:7][C:2]3[O:1][C:18]([C:15]4[CH:14]=[CH:13][N:12]=[CH:17][CH:16]=4)=[CH:10][C:9](=[O:11])[C:3]=3[CH:4]=2)[CH2:24][CH2:23]1

Participants

4

Reactant 3

HCID 102792-AcetylhydroquinoneHCID 79341Piperidin-4-olHCID 417436Pyridine-4-carbonyl chloride

Product 1

HCID 18959699HCID 18959699, compound

Procedure

The compound was prepared by the method of Example 11 from 2',5'-dihydroxyacetophenone, 4-pyridylcarbonyl chloride, and 4-hydroxypiperidine: mp 165°-166 ° C.

Sources & evidence

ORD record
ord-188cf4fadc4d4b1ea5ff5af3ac69b37a
Source dataset
uspto-grants-1994_01
Patent number
US05278174

Reaction notes

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