HRID1198129

反应详情

EQUATION

反应方程式

HRID 1198129 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In 50 ml of toluene were dissolved 3.8 g of 1-(4-difluoromethoxyphenyl)ethylamine and 2.3 g of triethylamine, and to the mixture was added 3.5 g of 6-(1-chloroethyl)-4,5-dichloropyrimidine. The mixture was refluxed under heating for 5 hours.

WORKUP

后处理

  1. temperatureThe mixture was refluxed
  2. temperatureunder heating for 5 hours