HRID1198552

反应详情

EQUATION

反应方程式

HRID 1198552 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

A solution of 1-[3-(1,3-dioxolan-2-yl)benzyl]-7-cyanomethoxyindole (50 mg., 0.15 mmol) in tetrahydrofuran (1 ml) and 2M hydrochloric acid (0.5 ml) was stirred at room temperature for 1 hour, diluted with water and extracted with ethyl acetate. The extract was dried and evaporated to a dark oil.

WORKUP

后处理

  1. extractionextracted with ethyl acetate
  2. customThe extract was dried
  3. customevaporated to a dark oil