Ammonium → 9-Bromo-2-iodo-5,6-dihydroimidazo[1,2-d][1,4]benzoxazepine

HRID 1222505Notes

Reaction equation

HRID 1222505 reaction equation
[Br-:1].[Br:5][c:6]1[cH:7][c:8]2[c:9]([cH:20][cH:21]1)-[c:10]1[n:11]([c:15]([I:19])[c:16]([I:18])[n:17]1)[CH2:12][CH2:13][O:14]2.[CH2:24]([O:25][CH2:26][CH3:27])[CH3:28].[CH2:29]1[O:30][CH2:31][CH2:32][CH2:33]1.[CH2:2]([Mg+:3])[CH3:4].[Cl-:22].[NH4+:23]>>[Br:5][c:6]1[cH:7][c:8]2[c:9]([cH:20][cH:21]1)-[c:10]1[n:11]([cH:15][c:16]([I:18])[n:17]1)[CH2:12][CH2:13][O:14]2

Participants

8

Reactant 7

HCID 223AmmoniumHCID 259Bromide ionHCID 312ChlorideHCID 3283Diethyl EtherHCID 8028TetrahydrofuranHCID 582047669-Bromo-5,6-dihydro-2,3-diiodoimidazo(1,2-d)(1,4)benzoxazepineHCID 178461628HCID 178461628, compound

Product 1

HCID 582048589-Bromo-2-iodo-5,6-dihydroimidazo[1,2-d][1,4]benzoxazepine

Sources & evidence

ORD record
ord-c5024465ce714afdbd7d76decb244701
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (5/10)

Reaction notes

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