HRID1244832

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID949

N,N-Dimethylaniline

C8H11N

HCID8471

Triethylamine

C6H15N

HCID21923172

未命名化合物

HCID57296158

[2-(4-Methylbenzene-1-sulfonyl)hydrazinylidene]acetyl chloride

C9H9ClN2O3S

PRODUCTS

生成物

HCID69533136

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID241

Benzene

C6H6

溶剂HCID1140

Toluene

C7H8

溶剂HCID6212

Chloroform

CHCl3

溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

In step four, the alcohol 4 is treated with glyoxylic acid chloride (p-toluenesulfonyl)hydrazone and N,N-dimethylaniline followed by triethylamine in a solvent such as methylene chloride, chloroform, benzene, or toluene to give the diazoacetate 5.