HRID1246717

反应详情

EQUATION

反应方程式

HRID 1246717 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Methyl 1-benzyl-4-hydroxy-4-piperidinecarboxylate in methanol was treated with Pd(OH)2 (20% on carbon, 500 mg) under a hydrogen atmosphere. The mixture was allowed to stir at room temperature for 12 hours, filtered, and the filtrate was concentrated under reduced pressure.

WORKUP

后处理

  1. filtrationfiltered
  2. concentrationthe filtrate was concentrated under reduced pressure