HRID1248517

反应详情

EQUATION

反应方程式

HRID 1248517 的结构方程式

PROCEDURE

实验过程

Following Example 5, 18.8 g (0.22M) of butyrolactone and 37 g (0.2M) of n-dodecylamine was heated for 24 hours. Distillation of the residue gave 40.7 g (80.3%) of 1-n-dodecylazacyclopentan-2-one; b.p. 165°-170°/0.5 mm.

WORKUP

后处理

  1. temperaturewas heated for 24 hours
  2. distillationDistillation of the residue