3'-Aminoacetophenone → HCID 673709, compound

HRID 1248807Notes

Reaction equation

HRID 1248807 reaction equation
[NH2:1][C:2]1[CH:3]=[C:4]([C:8](=[O:10])[CH3:9])[CH:5]=[CH:6][CH:7]=1.C(N(C(C)C)CC)(C)C.[CH:20]1([C:23](Cl)=[O:24])[CH2:22][CH2:21]1>ClCCl>[C:8]([C:4]1[CH:3]=[C:2]([NH:1][C:23]([CH:20]2[CH2:22][CH2:21]2)=[O:24])[CH:7]=[CH:6][CH:5]=1)(=[O:10])[CH3:9]

Participants

5

Reactant 3

HCID 74173'-AminoacetophenoneHCID 77637Cyclopropanecarbonyl chlorideHCID 81531Diisopropylethylamine

Product 1

HCID 673709HCID 673709, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

N-(3-Acetylphenyl)cyclopropanecarboxamide was prepared by the reaction of m-aminoacetophenone, diisopropylethylamine and cyclopropanecarboxylic acid chloride in dichloromethane.

Sources & evidence

ORD record
ord-adade0f70fc944d389aa65e92e9537f9
Source dataset
uspto-grants-1986_12
Patent number
US04626538

Reaction notes

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