反应详情

In the same manner as described in Example 53, methyl (3RS)-9-methyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylate (421 mg), triethylamine (365 mg), carbon disulfide (137 mg), methanol (20 ml) and 2-thenyl chloride (238 mg) are reacted and treated. The product is recrystallized from methanol to give the title compound (360 mg, 57.6%) as colorless prisms, m.p. 139°-140° C.

1. customare reacted
2. additiontreated
3. customThe product is recrystallized from methanol