Hydrogen Peroxide → Benzene, ethenyl-, polymer with 1,3-butadiene

HRID 1253255Notes

Reaction equation

HRID 1253255 reaction equation
[CH2:1]=[CH:2][CH:3]=[CH2:4].OO>C(O)(C)C>[CH2:1]=[CH:2][CH:3]=[CH2:4].[CH2:1]=[CH:2][C:3]1[CH:4]=[CH:3][CH:2]=[CH:1][CH:4]=1

Participants

4

Reactant 2

HCID 784Hydrogen PeroxideHCID 78451,3-Butadiene

Product 1

HCID 62697Benzene, ethenyl-, polymer with 1,3-butadiene

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

In an autoclave, with the atmosphere therein replaced with argon, were placed 75 g of 1,3-butadiene, 25 g of sytrene, 70 g of isopropyl alcohol, and 10 g of 60% hydrogen peroxide, followed by polymerization reaction at 90° C. for 5 hours. Thus there was obtained a butadiene-styrene copolymer.

Workup

  1. customfollowed by polymerization reaction at 90° C. for 5 hours

Sources & evidence

ORD record
ord-d7b66bf3a60549098b956d99456da4d9
Source dataset
uspto-grants-1988_05
Patent number
US04748212

Reaction notes

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