HRID1255526
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
产物
PROCEDURE
实验过程
A 100 mL round bottom flask was charged with the product of Step 6 (1.91 g, 5.05 mmol). Added HCl (4.0M in dioxane) (30 mL, 120 mmol). Stirred at room temperature for 1 hour. Evaporated. Added ethanol. Evaporated. Repeated. The title compound remained as a pale foam. (1.59 g, 5.05 mmol, 100% yield). LCMS (ES+) m/z 279.3 (M+H)+.
WORKUP
后处理
- customEvaporated
- customEvaporated