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HRID1255966

反应详情

EQUATION

反应方程式

HRID 1255966 的结构方程式

REACTANTS

反应物

4
结构：c1c[nH]cn1
HCID795

Imidazole

C3H4N2

结构：OCCOCCOCCOCCO
HCID8200

Tetraethylene glycol

C8H18O5

结构：CC(C)(C)[Si](C)(C)Cl
HCID28928

Chloro(1,1-dimethylethyl)dimethylsilane

C6H15ClSi

结构：CC(O)OCCO[Si](C)(C)C(C)(C)C
HCID86618841

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)[Si](C)(C)OCCOCCOCCOCCO
HCID14827669

13,13,14,14-Tetramethyl-3,6,9,12-tetraoxa-13-silapentadecan-1-ol

C14H32O5Si

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Compound 28b was prepared according to the procedure described hereinabove for Compound 28a, using tetraethylene glycol (6 grams, 30 mmol), TBDMSCl (3 grams, 20 mmol), and imidazole (1.4 grams, 20 mmol) in DMF (24 ml), yielding 3.79 grams of the product (41% yield).