HRID1258665

反应详情

EQUATION

反应方程式

HRID 1258665 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of N-(4-chloro-3-nitro-benzyl)-1-trifluoromethyl-cyclopropanecarboxamide (340 mg, 1.1 mmol), EtOAc (10 mL) and Ra—Ni (30 mg) was stirred at rt under a hydrogen atmosphere (3 bar). The catalyst was removed by filtration and the filtrate was concentrated to give the sub-title compound.

WORKUP

后处理

  1. customThe catalyst was removed by filtration
  2. concentrationthe filtrate was concentrated