Triethylamine → HCID 15589806, compound

HRID 1263181Notes

Reaction equation

HRID 1263181 reaction equation
[CH2:1]([P:3]([C:6]1[CH:11]=[C:10]([O:12][C:13]2[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][C:14]=2[Cl:20])[CH:9]=[CH:8][C:7]=1[N+:21]([O-:23])=[O:22])(=[O:5])[OH:4])[CH3:2].[CH3:24][C:25]([CH3:32])([CH3:31])[C:26]([O:28][CH2:29]Cl)=[O:27].C(N(CC)CC)C>CN(C=O)C>[CH2:1]([P:3]([C:6]1[CH:11]=[C:10]([O:12][C:13]2[CH:18]=[CH:17][C:16]([Cl:19])=[CH:15][C:14]=2[Cl:20])[CH:9]=[CH:8][C:7]=1[N+:21]([O-:23])=[O:22])(=[O:4])[O:5][CH2:29][O:28][C:26](=[O:27])[C:25]([CH3:32])([CH3:31])[CH3:24])[CH3:2]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 87885Chloromethyl pivalateHCID 20251660HCID 20251660, compound

Product 1

HCID 15589806HCID 15589806, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Following the procedures of Example 1, P-ethyl-2-nitro-5-(2,4-dichlorophenoxy)phenylphosphinic acid (0.30 g, 0.80 mmol) and chloromethyl 2,2-dimethylpropanoate (0.24 g, 1.6 mmol) are reacted together in the presence of triethylamine (0.23 ml) and DMF (3 ml) to give 2,2-dimethylpropionyloxymethyl P-ethyl-2-nitro-5-(2,4-dichlorophenoxy)phenylphosphinate.

Sources & evidence

ORD record
ord-9814606536414f80ab71d9731160086d
Source dataset
uspto-grants-1984_06
Patent number
US04456465

Reaction notes

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