Triethylamine → HCID 2781982, compound

HRID 1266517Notes

Reaction equation

HRID 1266517 reaction equation
[Cl:1][C:2]1[CH:8]=[C:7]([Cl:9])[CH:6]=[CH:5][C:3]=1[NH2:4].[Br:10][CH2:11][C:12](Br)=[O:13].C(N(CC)CC)C>C(Cl)Cl>[Br:10][CH2:11][C:12]([NH:4][C:3]1[CH:5]=[CH:6][C:7]([Cl:9])=[CH:8][C:2]=1[Cl:1])=[O:13]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 111232,4-DichloroanilineHCID 61147Bromoacetyl bromide

Product 1

HCID 2781982HCID 2781982, compoundYield 80.4%

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

This compound was prepared similarly to Example II-11 from 4.2 g of 2,4-dichloroaniline and 5.76 g of bromoacetyl bromide and 2.89 g of triethylamine in methylene chloride. This gave 5.9 g (80.4%) of the title compound.

Sources & evidence

ORD record
ord-6cabf7f308ab4303b407f96865b23db1
Source dataset
uspto-grants-2003_04
Patent number
US06548538B2

Reaction notes

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