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HRID1266960

反应详情

EQUATION

反应方程式

HRID 1266960 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：Cc1ccc(S(=O)(=O)N=[N+]=[N-])cc1
HCID13661

未命名化合物

结构：CC1=NN(c2ccc(C(=O)O)cc2)C(=O)C1
HCID109029

4-(3-Methyl-5-oxo-4,5-dihydro-1H-pyrazol-1-yl)benzoic acid

C11H10N2O3

PRODUCTS

生成物

1
结构：CC1=NN(c2ccc(C(=O)O)cc2)C(=O)C1=[N+]=[N-]
HCID135502619

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

A solution of 4-(3-methyl-5-oxo-2-pyrazolin-1-yl)benzoic acid (5.0 g, 0.023 mol) and p-toluenesulfonylazide (5.03 g, 0.026 mol) in methanol (30.0 mL) was treated with triethylamine (5.2 g; 0.051 mol.) and the reaction was stirred at room temperature for 5 hours.