HRID1268342

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID14487

Diisobutylaluminum hydride

C8H19Al

$结构：CCOC(=O)/C=C(\C)c1ccc(-c2cc(Br)cc(Br)c2)cc1$

HCID22557684

未命名化合物

PRODUCTS

生成物

$结构：C/C(=C\CO)c1ccc(-c2cc(Br)cc(Br)c2)cc1$

HCID69800831

未命名化合物

PROCEDURE

实验过程

The colourless gum (E)-3-(3′,5′-dibromo-biphenyl-4-yl)-but-2-en-1-ol was prepared by DIBAL-H reduction of (E)-ethyl 3-(3′,5′-dibromo-biphenyl-4-yl)-but-2-enoate as described for example 52b, with the purification of the product being carried out by preparative HPLC.

WORKUP

后处理

customas described for example 52b, with the purification of the product