HRID1270397

反应详情

EQUATION

反应方程式

HRID 1270397 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

tert-Butyl[3-(4-methoxypyrimidin-2-yl)-2-oxo-2,3-dihydro-1H-benzimidazol-1-yl]acetate from Step A (110 mg, 0.309 mmol) was dissolved in TFA (2 mL) and CH2Cl2 (2 mL) and the mixture was stirred at ambient temperature for 48 h, then concentrated in vacuo to give the title compound. MS: m/z=301 (M+1).

WORKUP

后处理

  1. concentrationconcentrated in vacuo