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HRID1271764

反应详情

EQUATION

反应方程式

HRID 1271764 的结构方程式

REACTANTS

反应物

3
结构：CCN(CC)CC
HCID8471

Triethylamine

C6H15N

结构：O=C(Cl)c1ccc2ccccc2c1
HCID75246

2-Naphthalenecarbonyl chloride

C11H7ClO

结构：Cn1c(C(F)(F)F)cc(=O)n(-c2ccc(Cl)cc2N)c1=O
HCID86585905

未命名化合物

PRODUCTS

生成物

1
结构：Cn1c(C(F)(F)F)cc(=O)n(-c2ccc(Cl)cc2NC(=O)c2ccc3ccccc3c2)c1=O
HCID57179635

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

A solution of 3-(2-amino-4-chlorophenyl)-1-methyl-6-trifluoromethyl-2,4(1H, 3H)-pyrimidinedione (0.4 g), 2-naphthoyl chloride (0.29 g) and triethyl amine (0.19 g) in anhydrous tetrahydro furan (30 ml) was heated at reflux temperature overnight under nitrogen atmosphere.

WORKUP

后处理

  1. temperatureat reflux temperature overnight under nitrogen atmosphere