HRID12727

反应详情

EQUATION

反应方程式

HRID 12727 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

3-(2,4-Dimethoxy-pyrimidin-5-yl)-pyridine-2-carbonitrile (Prep102, 1 g, 4.13 mmol) was dissolved in a solution of 4N HCl in dioxane (20 ml). The mixture was refluxed for 45 minutes. The solvent was removed under vacuum to give 1 g of the title compound (97% yield).

WORKUP

后处理

  1. temperatureThe mixture was refluxed for 45 minutes
  2. customThe solvent was removed under vacuum