huagongshe.com
HRID1278738

反应详情

EQUATION

反应方程式

HRID 1278738 的结构方程式

REACTANTS

反应物

3
结构：O=C(O)C1CCCN1
HCID614

DL-Proline

C5H9NO2

结构：CC(C)O
HCID3776

Isopropanol

C3H8O

结构：O=S(=O)(Cl)c1ccc(F)cc1
HCID9588

Benzenesulfonyl chloride, 4-fluoro-

C6H4ClFO2S

PRODUCTS

生成物

1
结构：CC(C)OC(=O)C1CCCN1S(=O)(=O)c1ccc(F)cc1
HCID69900402

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from DL-proline, isopropanol, and 4-fluorobezenesulfonyl chloride according to the procedure of Intermediate 48 as a clear oil; 1H NMR (CDCl3) δ 1.21-1.28 (m, 6H), 1.80-1.85 (m, 1H), 1.95-2.10 (m, 3H), 3.31-3.49 (m, 2H), 4.26-4.36 (m, 1H), 4.95-5.08 (m, 1H), 7.15-7.23 (m, 2H), 7.89-8.08 (m, 2H); MS (ES) m/z 315.8 (MH+); HRMS for C14H18FNO4S: 338.0830 (M+Na).