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HRID1283403

反应详情

EQUATION

反应方程式

HRID 1283403 的结构方程式

REACTANTS

反应物

2
结构：NN.O
HCID24654

Hydrazine hydrate (1:1)

H6N2O

结构：COc1ccc(C(=O)CCC(=O)O)cc1Cl
HCID10060312

Benzenebutanoic acid, 3-chloro-4-methoxy-gamma-oxo-

C11H11ClO4

PRODUCTS

生成物

1
结构：COc1ccc(C2=NNC(=O)CC2)cc1Cl
HCID10823876

未命名化合物

收率 84%

PROCEDURE

实验过程

This compound was prepared in 84% yield by reaction of 3-(3-chloro-4-methoxybenzoyl)propionic acid with hydrazine hydrate in ethanolic solution at reflux temperature for 5 hours. It had mp 194°-195°C after crystallisation from ethanol.

WORKUP

后处理

  1. temperatureat reflux temperature for 5 hours
  2. customafter crystallisation from ethanol