Benzamide → Benzamide

HRID 1285859Notes

Reaction equation

HRID 1285859 reaction equation
Brc1cccnc1.NC(=O)c1ccccc1>CC(C)(C)[P](c1ccc(N)cc1)(C(C)(C)C)->[Pd]1(<-[NH2]c2ccccc2-c2cccc[c]21)[O]S(C)(=O)=O.CN1CCCN2CCCN=C12.CS(C)=O>O=C(Nc1cccnc1)c1ccccc1

Participants

9

Reactant 2

HCID 2331BenzamideHCID 122863-Bromopyridine

Product 4

HCID 2331BenzamideHCID 7095BiphenylHCID 122863-BromopyridineHCID 293813N-pyridin-3-ylbenzamide

Reagents, catalysts & solvents 3

HCID 1235837-Methyl-1,5,7-triazabicyclo[4.4.0]dec-5-eneReagentHCID 178454868HCID 178454868, compoundReagentHCID 679Dimethyl SulfoxideSolvent4×

Procedure

The Mosquito was used to combine the source plate solutions by multi-aspiration of 250 nL of each of the four reaction components and then to dose the resulting reaction mixture (1 uL) into a 1536-well plate

Workup

  1. additionNo procedure recorded
  2. aliquotNo procedure recorded
  3. additionNo procedure recorded

Sources & evidence

ORD record
ord-74a708aacedd4a49add4e14f758191e8
Source dataset
HTE Pd-catalyzed cross-coupling screen
Original link
View source

Reaction notes

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