3-Bromopyridine → Biphenyl

HRID 1286152노트

반응식

HRID 1286152 반응식
Brc1cccnc1.N=C(N)Cc1ccccc1>C1CCC2=NCCCN2CC1.CC(C)c1cc(C(C)C)c(-c2ccccc2[P](C2CCCCC2)(C2CCCCC2)->[Pd]2(<-[NH2]c3ccccc3-c3cccc[c]32)[O]S(C)(=O)=O)c(C(C)C)c1.CS(C)=O>N=C(Cc1ccccc1)Nc1cccnc1

참가 물질

9

반응물 2

HCID 122863-BromopyridineHCID 27787Benzeneethanimidamide

생성물 4

HCID 7095BiphenylHCID 122863-BromopyridineHCID 27787BenzeneethanimidamideHCID 178510790HCID 178510790, 화합물

시약·촉매·용매 3

HCID 811841,8-Diazabicyclo(5.4.0)undec-7-ene시약HCID 178439017HCID 178439017, 화합물시약HCID 679Dimethyl Sulfoxide용매4회

실험 절차

The Mosquito was used to combine the source plate solutions by multi-aspiration of 250 nL of each of the four reaction components and then to dose the resulting reaction mixture (1 uL) into a 1536-well plate

후처리

  1. addition기록된 절차가 없습니다
  2. aliquot기록된 절차가 없습니다
  3. addition기록된 절차가 없습니다

출처 및 근거

ORD 기록
ord-f21b688e85ed4dbd9978afd505e12936
출처 데이터셋
HTE Pd-catalyzed cross-coupling screen
원본 링크
출처 보기

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