Azobisisobutyronitrile → HCID 86734082, compound

HRID 1287947Notes

Reaction equation

HRID 1287947 reaction equation
[CH2:1]([S:3][CH2:4][CH2:5][O:6][C:7](=[O:10])[CH:8]=[CH2:9])[CH3:2].[C:11]([NH2:15])(=[O:14])[CH:12]=[CH2:13].N(C(C)(C)C#N)=NC(C)(C)C#N>C(O)(C)C.O>[C:11]([NH2:15])(=[O:14])[CH:12]=[CH2:13].[CH2:1]([S:3][CH2:4][CH2:5][O:6][C:7](=[O:10])[CH:8]=[CH2:9])[CH3:2]

Participants

6

Reactant 3

HCID 6547AzobisisobutyronitrileHCID 6579AcrylamideHCID 27134Acrylic acid, 2-(ethylthio)ethyl ester

Product 1

HCID 86734082HCID 86734082, compound

Reagents, catalysts & solvents 2

HCID 962WaterSolventHCID 3776IsopropanolSolvent

Procedure

In a 2 liters reaction vessel fitted with stirrer, reflux condenser, nitrogen inlet tube and thermometer, 60 g of β-ethylthioethyl-acrylate, 140 g of acrylamide, 2 g of n-lauryl-mercaptan and 5 g of azo-bis-isobutyronitrile were dissolved in a mixture of 650 ml of isopropanol and 350 ml of water.

Workup

  1. customIn a 2 liters reaction vessel
  2. customfitted with stirrer
  3. temperaturereflux condenser, nitrogen inlet tube

Sources & evidence

ORD record
ord-72eecde51ed6414cb1a68952991fdfde
Source dataset
uspto-grants-1976_10
Patent number
US03986877

Reaction notes

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