HRID1294897

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID207836

Cyclohexylhydrazine--hydrogen chloride (1/1)

C6H15ClN2

HCID11471075

(3-chloro-2-fluorophenyl)-(4-methoxyphenyl)-methanone

C14H10ClFO2

PRODUCTS

生成物

结构：COc1ccc(-c2nn(C3CCCCC3)c3c(Cl)cccc23)cc1

HCID68885462

未命名化合物

收率 92%

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID14284

N,N-Dimethylpyridin-4-amine

C7H10N2

PROCEDURE

实验过程

Prepared according to Method C step A (3-chloro-2-fluorophenyl)-(4-methoxyphenyl)-methanone (0.55 g, 1.85 mmol), cyclohexylhydrazine hydrochloride (0.42 g, 2.7 mmol) and DMAP (0.225 g, 1.85 mmol) to give the product (0.58 g) as a yellow oil.

WORKUP

后处理

customPrepared