反应详情

To a solution of 3-(4-Formyl-phenoxymethyl)benzonitrile (1 equiv), in DMSO was added potassium carbonate (0.5 equiv), and hydrogen peroxide (4 equiv). The reaction mixture stirred at room temperature for 2 hours. The reaction was monitored by TLC. It was poured on water and extracted with ethyl acetate (×3). The organic phase was dried over magnesium sulphate, filtered and concentrated under vacuum to yield a white solid.

1. additionIt was poured on water
2. extractionextracted with ethyl acetate (×3)
3. dry with materialThe organic phase was dried over magnesium sulphate
4. filtrationfiltered
5. concentrationconcentrated under vacuum
6. customto yield a white solid