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HRID133758

反应详情

EQUATION

反应方程式

HRID 133758 的结构方程式

REACTANTS

反应物

2
结构：C=C(C)C(=O)Cl
HCID13528

Methacryloyl chloride

C4H5ClO

结构：Nc1ccc([N+](=O)[O-])c(CO)c1
HCID13238551

(5-Amino-2-nitrophenyl)methanol

C7H8N2O3

PRODUCTS

生成物

1
结构：C=C(C)C(=O)Nc1ccc([N+](=O)[O-])c(CO)c1
HCID67527004

N-[3-(Hydroxymethyl)-4-nitrophenyl]-2-methylprop-2-enamide

C11H12N2O4

PROCEDURE

实验过程

N-(3-Hydroxymethyl-4-nitrophenyl)-2-methylacrylamide was prepared as described in Example 1a starting from (5-Amino-2-nitrophenyl)methanol and methacryloyl chloride. 1H NMR (400 MHz, DMSO-d6): 1.97 (3H, s), 4.85 (2H, d, J=5.2 Hz), 5.56 (1H, t, J=5.2 Hz), 5.61 (1H, s), 5.90 (1H, s), 7.93 (1H, dd, J=9.0 Hz, J=2.1 Hz), 8.11 (1H, d, J=9.0 Hz), 8.20 (1H, d, J=2.1 Hz), 10.32 (1H, s).