反应详情

To a suspension of 0.4 g (10 mmol) of potassium hydride in tetrahydrofurane, 1.96 g (10 mmol) of a (3-trimethylsiloxy-propyl)-cyclopentadiene in tetrahydrofurane is added. The reaction is maintained under stirring for 2 hours. Subsequently, the resulting suspension is concentrated to dryness, leaving an oily solid that, when it is washed with hexane, gives a cream-coloured solid. (1.6 g, 7 mmol. Yield:70%).

1. additionis added
2. temperatureThe reaction is maintained
3. concentrationSubsequently, the resulting suspension is concentrated to dryness
4. customleaving an oily solid that, when it
5. washis washed with hexane
6. customgives a cream-coloured solid