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HRID1354677

反应详情

EQUATION

反应方程式

HRID 1354677 的结构方程式

REACTANTS

反应物

6
结构：Nc1ccc(Oc2ccccc2)cc1
HCID8764

Benzenamine, 4-phenoxy-

C12H11NO

结构：O=[N+]([O-])c1ccc(F)cc1
HCID9590

1-Fluoro-4-nitrobenzene

C6H4FNO2

结构：O=C(n1ccnc1)n1ccnc1
HCID68263

1,1'-Carbonylbis(1H-imidazole)

C7H6N4O

结构：CN(C)C1CCNCC1
HCID417391

N,N-Dimethylpiperidin-4-amine

C7H16N2

结构：CN(C)C1CCN(c2ccc(N)cc2)CC1
HCID10889414

1-(4-aminophenyl)-N,N-dimethylpiperidin-4-amine

C13H21N3

结构：[H][H]
HCID178418361

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)C1CCN(c2ccc(NC(=O)Nc3ccc(Oc4ccccc4)cc3)cc2)CC1
HCID10320492

未命名化合物

PROCEDURE

实验过程

Dimethylpiperidin-4-ylamine was reacted with 4-fluoronitrobenzene, the resulting nitro compound was reduced with hydrogen and finally the aniline ([1-(4-aminophenyl)piperidin-4-yl]dimethylamine) was reacted with CDI and 4-phenoxyaniline by method A, B and C. This resulted in the product with the molecular weight of 430.55 (C26H30N4O2); MS (ESI): 431 (M+H+).

WORKUP

后处理

  1. customThis resulted in the product with the molecular weight of 430.55 (C26H30N4O2)